4-Bromo-N-(di-n-propylcarbamothioyl)benzamide
نویسندگان
چکیده
منابع مشابه
4-Bromo-N-(di-n-propylcarbamothioyl)benzamide
The synthesis of the title compound, C(14)H(19)BrN(2)OS, involves the reaction of 4-bromo-benzoyl chloride with potassium thio-cyanate in acetone followed by condensation of the resulting 4-bromo-benzoyl isothio-cyanate with di-n-propyl-amine. Typical thio-urea carbonyl and thio-carbonyl double bonds, as well as shortened C-N bonds, are observed in the title compound. The short C-N bond lengths...
متن کامل4-Bromo-N-phenylbenzamide
The mol-ecule of the title benzamide derivative, C(13)H(10)BrNO, is twisted with the dihedral angle between the phenyl and 4-bromo-phenyl rings being 58.63 (9)°. The central N-C=O plane makes dihedral angles of 30.2 (2) and 29.2 (2)° with the phenyl and 4-bromo-phenyl rings, respectively. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds into chains along [100]. C-H⋯π contacts combi...
متن کامل4-Bromo-N-phenylaniline
In the title compound, C(12)H(10)BrN, the dihedral angle between the benzene rings is 52.5 (1)°, whereas the pitch angles, or the angles between the mean plane of each aryl group 'propeller blade' and the plane defined by the aryl bridging C-N-C angle, are 19.6 (2) and 36.2 (3)°. While the N-H group is not involved in hydrogen-bonding inter-actions, the structure exhibits a network of inter-mol...
متن کامل4-Bromo-N-cyclohexylbenzenesulfonamide
The title compound, C(12)H(16)BrNO(2)S, adopts an L-shaped conformation with the central C-S-N-C torsion angle being -77.8 (3)°. The crystal packing features N-H⋯O hydrogen bonds, which lead to C(4) chains propagating in [010]; the second O atom is involved in short intra-molecular C-H⋯O contacts.
متن کامل4-Bromo-N-phenylbenzamidoxime
The title compound, C(13)H(11)BrN(2)O, a hydroxy-amidine derivative (an amidoxime), was obtained by addition of the corresponding imidoyl chloride to hydroxy-lamine. The benzene and phenyl rings are twisted from the mean plane of the hydroxy-amidine group by 34.4 (1) and 59.2 (1)°, respectively. In the crystal structure, inter-molecular O-H⋯N hydrogen bonds link pairs of mol-ecules, forming cen...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2009
ISSN: 1600-5368
DOI: 10.1107/s1600536809003511